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this post was submitted on 30 Mar 2025
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TechTakes
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Sheesh. Everyone knows you keep the phenethylamines inside the fridge proper, not on the door, where the temperature is less stable. (Source: the Shulgins' Kitchen Procedures I Have Known And Loved.)
@blakestacey I believe there was rapid turnover. (PIHKAL was cited as the cookbook being used. This was in 1993, so it was pretty new …)
now you've got me thinking if storage in fridge is necessary at all, if these are salts. worst thing that can reasonably happen is that salt picks up some water from the air, on top of water condensing on sample when vial was opened while still cold. freebase would probably be air-sensitive, but for compounds that are known sensitive i'd put them under argon/nitrogen, tape vial shut (with normal electrical tape, not parafilm) and store in freezer instead. sigma lists storage temperature for MDMA analytical standard (weak solution of freebase in methanol) as -20C, but some of this might be legal cover with excess requirements for cases where you'd have to be absolutely sure that analytical standard didn't decompose (like in evidence in drug cases)